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Scanning Electron Microscopy (SEM) for Materials Characterization

Scanning Electron Microscopy (SEM)Scanning Electron Microscopy (SEM) is one of the most fundamental tools of the failure analysis lab. The ability to examine even the most minute of details at high resolution is crucial, especially when a given defect might be only a few nanometers wide. As integrated circuit processes continue to shrink, the use of a SEM becomes a necessity, as features shrink below the smallest size that can be resolved with optical wavelengths of light. SEM is by no means limited to imaging failures on integrated circuits, however; with the proper techniques, the SEM can also be a powerful tool for material characterization.

Generally, scanning electron microscopy uses the secondary electrons generated by bombarding a sample with an electron beam to generate an image. This secondary electron image can be used with a certain degree of interpretation as an implied topographical shot - things like surface roughness and uniformity can be qualitatively examined. Additionally, a secondary electron image will often show differences in the conductivities of materials, due to the charging effects observed as the beam scans across the surface of the part; this can be useful for identifying contaminants on the surface of a device. In addition to these techniques, there are other applications for the SEM that can provide contrast based on the materials present on a device.

When backscattered electrons are collected instead of secondary electrons, the scanning electron microscope can provide an entirely different view of the same sample. When generating a backscatter image, contrast is determined elementally; the further apart two elements appear on the periodic table, the higher the contrast will be between them on the SEM image. Using backscatter images to identify elemental changes can be a useful precursor for more in-depth chemical analysis like energy dispersive spectroscopy; being able to visually see material changes can greatly influence the sites chosen for a more in-depth look.

By no means are these two rudimentary scanning electron microscope operating modes the only techniques available for examining devices or materials. Changing accelerating voltages and currents, applying outside stimuli (like voltage pulses), or examining a material under different levels of vacuum can all create vastly different SEM images. Being able to generate an image is only half of the battle, however; it is still crucial to know which images are the most valuable, and how to select a given imaging mode based on the needs of the analysis.

Derek Snider is a failure analyst at Insight Analytical Labs, where he has worked since 2004. He is currently an undergraduate student at the University of Colorado, Colorado Springs, where he is pursuing a Bachelors of Science degree in Electrical Engineering.

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